HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Butyric acid (4-quinolinylmethylene)hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Butyrohydrazide | HCID 77079 | — |
| Reactant | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| Solvent | Water | HCID 962 | — |
| Product | Butyric acid (4-quinolinylmethylene)hydrazide | HCID 86743403 | 85.4% |
Reaction Steps
A mixture of 7.85 gm (0.05 mole) of 4-quinolinecarboxaldehyde, 5.11 gm (0.05 mole) of butyric acid hydrazide and 100 ml of ethanol is refluxed 4 hr. The reaction mixture is diluted with water and cooled to room temperature. The mixture is chilled. The solid that separates is collected, washed with water and dried to give 10.3 gm of the title compound, having a melting point of 130.4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870082 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-86b41a2e023d46cfa519dc8f0d867f61 |
| Source note | uspto-grants-1989_09 |