Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Quinolinecarboxaldehyde → HCID 54189210, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Quinolinecarboxaldehyde | HCID 79619 | — |
| 반응물 | m-Toluohydrazide | HCID 83082 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 54189210 | HCID 54189210 | 36.2% |
반응 단계
A mixture of 3.3 gm (0.021 mole) of 2-quinolinecarboxaldehyde, 3.15 gm (0.021 mole) of m-toluic acid hydrazide and 150 ml of absolute ethanol is refluzed 10 hr. The hot solution is filtered then diluted with water until cloudy. The mixture is cooled to room temperature and then chilled. The solid is collected to give 2.2 gm (36%) of the title compound having a melting point of 187.5°-188° C. after recrystallizing from methylene chloride/diethyl ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04870082 |
| 출처 데이터셋 | uspto-grants-1989_09 |
| ORD ID | ord-7d855082c6a547da820846c7f6518b6e |
| 출처 메모 | uspto-grants-1989_09 |