HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Quinolinecarboxaldehyde → HCID 53891208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Quinolinecarboxaldehyde | HCID 79619 | — |
| Reactant | o-Nitrobenzohydrazide | HCID 3781218 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53891208 | HCID 53891208 | 32.4% |
Reaction Steps
A mixture of 2.99 gm (0.019 mole) of 2-quinolinecarboxaldehyde, 3.44 gm (0.019 mole) of o-nitrobenzhydrazide and 150 ml of absolute ethanol is refluxed 9 hrs. The solvent is evaporated in vacuo. The solid is crystallized from methanol to give 1.97 gm (32%) of title compound, having a melting point of 195°-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870082 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-e78fc607e6a9449887cc0a61b5f3127a |
| Source note | uspto-grants-1989_09 |