Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Chloro-2-propen-1-ol | HCID 80076 | — |
| Product | HCID 86743408 | HCID 86743408 | — |
Reaction Steps
Oxalyl chloride (130 ml, 1.49 mol) was placed in a dry 3-neck flask under N2 and cooled to 0° C. With stirring, 2-chloroallyl alcohol (138 g, 1.49 mol) was added dropwise in a manner which maintained the temperature at 0°-2° C. and controlled the vigorous evolution of HCl, then allowed to warm to room temperature and held 16 hours and distilled to yield title product, 214 g, b.p. 82°-84° C./23 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04870170 |
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| Source dataset | uspto-grants-1989_09 |
|---|
| ORD ID | ord-1cd45196dfc348fc9e635b564ba174cb |
|---|
| Source note | uspto-grants-1989_09 |
|---|
