HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54406554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Reactant | HCID 54064055 | HCID 54064055 | — |
| Product | HCID 54406554 | HCID 54406554 | — |
Reaction Steps
14.1 g of the compound from (e), 10.7 g of ethyl orthoformate and 12.3 g of acetic anhydride are boiled for 2 hours. The volatile components are then removed by distillation first in a water-pump vacuum and then in a high vacuum at a bath temperature of 130° C. 14 g of the title compound remain (oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870182 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-318773cb8693402d8646bc0c3b64db3a |
| Source note | uspto-grants-1989_09 |