Dicyclohexylcarbodiimide → HCID 72739626, compound

Participants

Reaction Steps

To a solution of tri-n-butylstannyl 5-(tri-n-butylstannyl)-4-pentenoate acid (1.0 equiv.) in anhydrous THF at room temperature is added dicyclohexyl carbodiimide (1.2 equiv) (Aldrich) and 2,3,5,6-tetrafluorophenol (1.2 equiv) (Aldrich). The resulting solution is stirred overnight. The mixture is filtered, the filtrate is concentrated, and the residue is chromatographed to provide 2,3,5,6-tetrafluorophenyl 5-(tri-n-butylstannyl)-4-pentenoate.

Provenance & Evidence