Dimethyl 1,4-cyclohexanedicarboxylate → Methyl Decanoate
Reaction equation
[C:1]1(CO)(CO)[CH2:6]CCC[CH2:2]1.C1(CO)CCC(CO)CC1.[CH:21]1([C:31]([O:33][CH3:34])=[O:32])[CH2:26][CH2:25][CH:24](C(OC)=O)[CH2:23][CH2:22]1>>[O:33]([CH3:34])[C:31]([CH2:21][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:2][CH2:1][CH3:6])=[O:32]Participants
4
Procedure
A process according to claim 20, in which the cyclohexanedimethanol is 1,4-cyclohexanedimethanol, the dialkyl cyclohexanedicarboxylate is dimethyl 1,4-cyclohexanedicarboxylate, the hydrogenation zone is maintained at a temperature of from about 200° C. to about 260° C. and a pressure of from about 450 psia (about 31.03 bar) to about 1000 psia (about 68.95 bar).
Workup
- temperaturethe hydrogenation zone is maintained at a temperature of from about 200° C. to about 260° C.
Sources & evidence
- ORD record
- ord-738746397e3349c5b50ae5e735fdee00
- Source dataset
- uspto-grants-1995_03
- Patent number
- US05395990
Reaction notes
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