Boron tribromide → HCID 67277611, compound

HRID 16088Notes

Reaction equation

HRID 16088 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:15]2[CH:20]=[C:19]([Cl:21])[CH:18]=[CH:17][C:16]=2[O:22]C)[CH:5]=[CH:6][C:7]=1[C:8]([N:10]1[CH2:14][CH2:13][CH2:12][CH2:11]1)=[O:9].B(Br)(Br)Br>C(Cl)Cl>[Cl:1][C:2]1[CH:3]=[C:4]([C:15]2[CH:20]=[C:19]([Cl:21])[CH:18]=[CH:17][C:16]=2[OH:22])[CH:5]=[CH:6][C:7]=1[C:8]([N:10]1[CH2:11][CH2:12][CH2:13][CH2:14]1)=[O:9]

Participants

4

Reactant 2

HCID 25134Boron tribromideHCID 67277288HCID 67277288, compound

Product 1

HCID 67277611HCID 67277611, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product from step b) (0.6 g) was dissolved in DCM (20 ml) and treated with boron tribromide (7 ml) and stirred for 1 h. Ice was added and a solid formed, which was filtered to give the sub-title compound. Yield 0.46 g.

Workup

  1. additionIce was added
  2. customa solid formed
  3. filtrationwhich was filtered

Sources & evidence

ORD record
ord-51beddb42f9c45a4a65e875cd1bd4edd
Source dataset
uspto-grants-2010_06
Patent number
US07737135B2

Reaction notes

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