反应详情

The titled compound was prepared substantially in accordance with the method detailed in Example 11 using 1.50 g (0.00651 mol) of 2-amino-N-[2-(1H-imidazol-2-yl)ethyl]benzamide, prepared as in Example 6A, and 3.76 g (0.01738 mol) of p-phenylbenzoyl chloride, with the exception that after removing ethyl acetate the final product was recrystallized from an ethyl acetate/methanol solution to provide 1.74 g of the desired titled compound (m.p. 197°-201° C.).

1. customThe titled compound was prepared substantially in accordance with the method
2. customthat after removing ethyl acetate the final product
3. customwas recrystallized from an ethyl acetate/methanol solution