HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → 3-[Benzyl-(2-Methoxycarbonyl-Ethyl)-Amino]-Propionic Acid Methyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[Benzyl-(2-Methoxycarbonyl-Ethyl)-Amino]-Propionic Acid Methyl Ester | HCID 69926 | — |
Reaction Steps
107 g of benzylamine in 200 ml of ethanol are cooled in an ice bath and 172.2 g of methyl acrylate in 250 ml of ethanol are slowly added. After 13 days at RT, the solvent is evaporated under vacuum and a part of the oily residue is then distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05397801 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-a980c0951db94c12a97b5f455f3b4abd |
| Source note | uspto-grants-1995_03 |