HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Phenol, 4-(2,2-dichloro-3-phenylcyclopropyl)-, acetate, trans-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 67724664 | HCID 67724664 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Phenol, 4-(2,2-dichloro-3-phenylcyclopropyl)-, acetate, trans- | HCID 67724570 | — |
Reaction Steps
The reaction of 1,1-dichloro-trans-2-(p-hydroxyphenyl)-3-phenylcyclopropane (Compound 17) (0.005 mol) and 0.4 mL of acetyl chloride yielded off-white needles (0.37 g, 22%) from EtOH, mp 124.5°-125.5° C. 1H NMR (CDCl3) δ 2.32 (s, 3H, OCOCH3), 3.20 (s, 2H, ArCH), 6.80-7.58 (m, 9H, ArH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05397802 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-ecc1bd03f5ae445baac0615c6be2e08e |
| Source note | uspto-grants-1995_03 |