Decyloxybenzoic acid → 6-(5-Ethoxy-2,2,3,3,4,4-hexafluoropentoxy)-2-hydroxynapthalene decyloxybenzoate

HRID 1608908Notes

Reaction equation

[CH2:1]([O:3][CH2:4][C:5]([F:26])([F:25])[C:6]([F:24])([F:23])[C:7]([F:22])([F:21])[CH2:8][O:9][C:10]1[CH:11]=[C:12]2[C:17](=[CH:18][CH:19]=1)[CH:16]=[C:15]([OH:20])[CH:14]=[CH:13]2)[CH3:2].[CH2:27]([O:37][C:38]1[CH:46]=[CH:45][CH:44]=[CH:43][C:39]=1[C:40]([OH:42])=[O:41])[CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>>[CH2:27]([O:37][C:38]1[CH:46]=[CH:45][CH:44]=[CH:43][C:39]=1[C:40]([OH:42])=[O:41])[CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].[CH2:1]([O:3][CH2:4][C:5]([F:25])([F:26])[C:6]([F:23])([F:24])[C:7]([F:21])([F:22])[CH2:8][O:9][C:10]1[CH:11]=[C:12]2[C:17](=[CH:18][CH:19]=1)[CH:16]=[C:15]([OH:20])[CH:14]=[CH:13]2)[CH3:2]

Participants

Reactant 2

HCID 18964568Decyloxybenzoic acid

HCID 200827456-(5-Ethoxy-2,2,3,3,4,4-hexafluoropentoxy)-2-hydroxynapthalene

Product 1

HCID 867485616-(5-Ethoxy-2,2,3,3,4,4-hexafluoropentoxy)-2-hydroxynapthalene decyloxybenzoate

Procedure

6-(5-Ethoxy-2,2,3,3,4,4-hexafluoropentoxy)-2-hydroxynapthalene decyloxybenzoate (Compound 9, Table 1) was prepared by esterification of 6-(5-ethoxy-2,2,3,3,4,4-hexafluoropentoxy)-2-hydroxynapthalene (prepared essentially as in Example 7) with decyloxybenzoic acid.

Sources & evidence

ORD record: ord-0cda872032204afc8d9cb11e2e41a2ca
Source dataset: uspto-grants-1995_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05399291

Reaction notes

Loading…