HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → HCID 22327697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | Triethanolamine | HCID 7618 | — |
| Catalyst | Phenothiazine | HCID 7108 | — |
| Solvent | P-Xylene | HCID 7809 | — |
| Product | HCID 22327697 | HCID 22327697 | 85% |
Reaction Steps
Example 1A was repeated using triethanolamine (59.6 g), phenothiazine (1 g), methacrylic acid (206 g), and methanesulfonic acid (57 g) in 200 ml p-xylene. Isolation by chromatography over basic alumina gave 120 g (85% yield) of triethanolamine trimethacrylate, which was 99.0% pure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399460 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-411d9ae2732a4200bcf20facae0f37d9 |
| Source note | uspto-grants-1995_03 |