HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20083125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 20083184 | HCID 20083184 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20083125 | HCID 20083125 | 38.1% |
Reaction Steps
120 mg of the compound (171) obtained in Example 48 was added to a mixture solution of 3 ml of tetrahydrofuran, 1 ml of 6N hydrochloric acid and 1 ml of water, and the solution was stirred for four days at room temperature. The deposited solid matter was filtered off and washed with water and ethanol in this order to obtain 44 mg of the subject compound (172).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399553 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-1006e9c0f0f6454ab6a781ad8c63e829 |
| Source note | uspto-grants-1995_03 |