Cysteamine → HCID 21733325, compound

Participants

Reaction Steps

100 mg of compound (8) obtained in Example 3 (1), 56 mg of 2-amino-ethanethiol and 109 mg of triethylamine were added to 2 ml of acetonitrile, and the solution was heated at reflux for 2 hours. After air-cooling, the solvent was removed by distillation. To the residue, ethanol was added, and the deposited solids were filtered off and washed with ether to obtain 60 mg of the subject compound (184).

Provenance & Evidence