Benzyl Alcohol → HCID 22924283, compound

HRID 1609168Notes

Reaction equation

HRID 1609168 reaction equation
[CH2:1](O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[F:9][Sb-:10]([F:15])([F:14])([F:13])([F:12])[F:11].[N:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(#N)C>[F:9][Sb-:10]([F:15])([F:14])([F:13])([F:12])[F:11].[CH2:1]([N+:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 244Benzyl AlcoholHCID 86748578HCID 86748578, compound

Product 1

HCID 22924283HCID 22924283, compoundYield 40%

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

10.81 g (0.1 mol) of benzyl alcohol and 31.58 g (0.1 mol) of pyridine hexafluoroantimonate were dissolved in 80 g of acetonitrile and allowed to react at 80° C. for 8 hours. After the completion of the reaction, the mixture was concentrated, and the precipitated white solid was washed with ether and dried to give N-benzylpyridinium hexafluoroantimonate. Yield: 40%.

Workup

  1. customto react at 80° C. for 8 hours
  2. customAfter the completion of the reaction
  3. concentrationthe mixture was concentrated
  4. washthe precipitated white solid was washed with ether
  5. customdried

Sources & evidence

ORD record
ord-a5b132045b324575800487cb9f8ebf41
Source dataset
uspto-grants-1995_03
Patent number
US05399695

Reaction notes

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