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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1609205Generated: October 30, 2026

Tributyltin azide → HCID 178459843, compound

https://huagongshe.com/reaction/1609205

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributyltin azideHCID 4984872—
ReactantHCID 22852222HCID 22852222—
ReactantHCID 178459842HCID 178459842—
ProductHCID 178459843HCID 178459843—

Reaction Steps

N-Carbopropoxy-N-[(2'-(1H-tetrazol-5-yl)biphenyl-4-yl)methyl]-(L)-valine benzyl ester starting from 1.04 g of N-carbopropoxy-N-[(2'-cyanobiphenyl-4-yl)methyl]-(L)-valine benzyl ester and 1.1 g of tributyltin azide and subsequent flash chromatography using the system N6. Amorphous product, TLC (system N6) Rf : 0.21.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05399578
Source datasetuspto-grants-1995_03
ORD IDord-8e4f4e596b7e48fc89ea5d9650d7e44b
Source noteuspto-grants-1995_03