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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1609206Generated: October 31, 2026

Tributyltin azide → HCID 178453030, compound

https://huagongshe.com/reaction/1609206

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributyltin azideHCID 4984872—
ReactantHCID 22852218HCID 22852218—
ReactantHCID 178453029HCID 178453029—
ProductHCID 178453030HCID 178453030—

Reaction Steps

N-Carbobutoxy-N-[(2'-(1H-tetrazol-5-yl)biphenyl-4-yl)methyl]-(L)-valine benzyl ester starting from 1.05 g of N-carbobutoxy-N-[(2'-cyanobiphenyl-4-yl)methyl]-(L)-valine benzyl ester and 1.05 g of tributyltin azide and subsequent flash chromatography using the system N6. Amorphous product. TLC (system N6) Rf : 0.17.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05399578
Source datasetuspto-grants-1995_03
ORD IDord-952b37c4039c4f18aa50e54d5e644a72
Source noteuspto-grants-1995_03