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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1609207Generated: October 30, 2026

Tributyltin azide → HCID 178502072, compound

https://huagongshe.com/reaction/1609207

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributyltin azideHCID 4984872—
ReactantHCID 53895507HCID 53895507—
ReactantHCID 178502071HCID 178502071—
ProductHCID 178502072HCID 178502072—

Reaction Steps

N-Carbomethoxy-N-[(2'-(1H-tetrazol-5-yl)biphenyl-4-yl)methyl]-(L)-valine benzyl ester starting from 3.21 g of N-carbomethoxy-N-[(2 '-cyanobiphenyl-4-yl)methyl]-(L)-valine benzyl ester and 3.50 g of tributyltin azide and subsequent flash chromatography using the system N6. Amorphous product, TLC (system N6) Rf : 0.26.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05399578
Source datasetuspto-grants-1995_03
ORD IDord-7dd5afe9bc3b410eaf0676c2b9de79d9
Source noteuspto-grants-1995_03