Trimethylsilyl isocyanate → HCID 19747660, compound

HRID 1609236Notes

Reaction equation

HRID 1609236 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][O:12][C:13]1[CH:18]=[CH:17][C:16]([C:19]2([CH2:26][NH:27][OH:28])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]2)=[CH:15][CH:14]=1.C[Si]([N:33]=[C:34]=[O:35])(C)C>>[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][O:12][C:13]1[CH:14]=[CH:15][C:16]([C:19]2([CH2:26][N:27]([OH:28])[C:34]([NH2:33])=[O:35])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]2)=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 70696Trimethylsilyl isocyanateHCID 20084231HCID 20084231, compound

Product 1

HCID 19747660HCID 19747660, compound

Procedure

In analogy to the procedure of Example 2, the title compound is prepared from 2.3 g (6.11 mmol) of the compound from Example XV and 0.77 g (6.68 mmol) of trimethylsilyl isocyanate.

Sources & evidence

ORD record
ord-696f14b5b03c49eeb5a9ed6c20b94eac
Source dataset
uspto-grants-1995_03
Patent number
US05399698

Reaction notes

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