HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 261393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 1-(2-fluoro-6-hydroxyphenyl)ethanone | HCID 2737324 | — |
| Product | HCID 261393 | HCID 261393 | — |
Reaction Steps
4 is prepared from 2-fluoro-6-hydroxyacetophenone (see Example 6) and benzoyl chloride by the procedure of Example 1. The material is purified by flash chromatography (eluting with 25% ethyl acetate in hexane), yielding 4 with a melting point of 144°-145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399584 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-73d806d333a54d9ba4ba5a546355d491 |
| Source note | uspto-grants-1995_03 |