HCID 178466632, compound → HCID 178466631, compound

HRID 1609265Notes

Reaction equation

HRID 1609265 reaction equation
[N+:1]([C:4]1[CH:24]=[CH:23][CH:22]=[CH:21][C:5]=1[O:6][C:7]1[CH:8]=[C:9]([CH:18]=[CH:19][CH:20]=1)[O:10][CH:11]([C:13]1[NH:17][N:16]=[N:15][N:14]=1)[CH3:12])([O-])=O>C(O)C.[C].[Pd]>[NH:17]1[C:13]([CH:11]([O:10][C:9]2[CH:8]=[C:7]([CH:20]=[CH:19][CH:18]=2)[O:6][C:5]2[CH:21]=[CH:22][CH:23]=[CH:24][C:4]=2[NH2:1])[CH3:12])=[N:14][N:15]=[N:16]1

Participants

4

Reactant 1

HCID 178466632HCID 178466632, compound

Product 1

HCID 178466631HCID 178466631, compound

Reagents, catalysts & solvents 2

HCID 178418390HCID 178418390, compoundCatalystHCID 702EthanolSolvent

Procedure

In 30 ml of ethanol was dissolved 5-[1-[3-(2-nitrophenoxy)phenoxy]ethyl]-1H-tetrazole and catalytic hydrogenation was carried out in the presence of 0.3 g of palladium-carbon at atmospheric temperature and pressure. After the reaction, the catalyst was filtered off and the filtrate was concentrated to give 2.1 g of the title compound as a brown oil.

Workup

  1. customAfter the reaction
  2. filtrationthe catalyst was filtered off
  3. concentrationthe filtrate was concentrated

Sources & evidence

ORD record
ord-9afe38bbdf3a4bb69d95588cc05a742c
Source dataset
uspto-grants-1995_03
Patent number
US05399703

Reaction notes

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