HRID1609265

反应详情

EQUATION

反应方程式

HRID 1609265 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

In 30 ml of ethanol was dissolved 5-[1-[3-(2-nitrophenoxy)phenoxy]ethyl]-1H-tetrazole and catalytic hydrogenation was carried out in the presence of 0.3 g of palladium-carbon at atmospheric temperature and pressure. After the reaction, the catalyst was filtered off and the filtrate was concentrated to give 2.1 g of the title compound as a brown oil.

WORKUP

后处理

  1. customAfter the reaction
  2. filtrationthe catalyst was filtered off
  3. concentrationthe filtrate was concentrated