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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1609290Erstellt: 25. Oktober 2026

Sodium → HCID 178444960, Verbindung

https://huagongshe.com/reaction/1609290

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSodiumHCID 5360545—
EduktHCID 178444959HCID 178444959—
LösungsmittelEthanolHCID 702—
LösungsmittelDiethyl EtherHCID 3283—
ProduktHCID 178444960HCID 17844496092,5%

Reaktionsschritte

In 30 ml of ether was dissolved 2.0 g of N-[2-[3-[1-(1H-tetrazol-5-yl)ethoxy]phenoxy]phenyl]-4-hexyloxybenzamide followed by addition of a solution of 90 mg of sodium in ethanol, and the mixture was concentrated in vacuo to dryness. After addition of isopropyl ether, the resulting foamy solid was pulverized, filtered and dried to give 1.9 g of the sodium salt as a white amorphous powder.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05399703
Quelldatensatzuspto-grants-1995_03
ORD IDord-d1a9acbae6d7492d8361972f84ec0462
Quellennotizuspto-grants-1995_03