HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium → HCID 178444960, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium | HCID 5360545 | — |
| Edukt | HCID 178444959 | HCID 178444959 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | HCID 178444960 | HCID 178444960 | 92,5% |
Reaktionsschritte
In 30 ml of ether was dissolved 2.0 g of N-[2-[3-[1-(1H-tetrazol-5-yl)ethoxy]phenoxy]phenyl]-4-hexyloxybenzamide followed by addition of a solution of 90 mg of sodium in ethanol, and the mixture was concentrated in vacuo to dryness. After addition of isopropyl ether, the resulting foamy solid was pulverized, filtered and dried to give 1.9 g of the sodium salt as a white amorphous powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05399703 |
| Quelldatensatz | uspto-grants-1995_03 |
| ORD ID | ord-d1a9acbae6d7492d8361972f84ec0462 |
| Quellennotiz | uspto-grants-1995_03 |