HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22852344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 22852343 | HCID 22852343 | — |
| Product | HCID 22852344 | HCID 22852344 | — |
Reaction Steps
A mixture of 1 g of 2-[2-((4S,5S)-3-BOC-4-cyclohexylethyl-2,2-dimethyl-5-oxazolidinyl)-ethyl]-2-ethoxycarbonyl-1,3-dithiane 1,1,3,3-tetroxide, 50 ml of dioxane and 20 ml of 2 N NaOH (aqueous) is stirred at 20° for 3 h. The usual working up gives 2-[2-((4S,5S)-3-BOC-4-cyclohexylmethyl-2,2-dimethyl-5-oxazolidinyl)-ethyl]-2-carboxy-1,3-dithiane 1,1,3,3-tetroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401722 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-718289154a494899b3784a3bc897e370 |
| Source note | uspto-grants-1995_03 |