HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydro-4H-pyran-4-one → HCID 14985860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydro-4H-pyran-4-one | HCID 121599 | — |
| Reactant | 1-(Benzyloxy)-3-bromobenzene | HCID 2756638 | — |
| Product | HCID 14985860 | HCID 14985860 | 77% |
Reaction Steps
Using the Grignard reaction procedure described in the portion of Example 1 which is concerned with the preparation of starting materials, 3-benzyloxybromobenzene was reacted with tetrahydropyran-4-one to give 4-(3-benzyloxyphenyl)-4-hydroxytetrahydropyran in 77% yield, m.p. 84°-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401751 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-a68d661f016d4f39bc594954dec5a8c3 |
| Source note | uspto-grants-1995_03 |