HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 57284075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 57113227 | HCID 57113227 | — |
| Product | HCID 57284075 | HCID 57284075 | 95% |
Reaction Steps
Using the procedure described in Example 11, 4-[3-(1,2-dihydro-1-methyl-2-oxoquinolin-6-ylmethoxy)-5-trifluoromethylphenyl]-4-hydroxytetrahydropyran was reacted with methyl iodide to give 4-[3-(1,2-dihydro-1-methyl-2-oxoquinolin-6-ylmethoxy)-5trifluoromethylphenyl]-4-methoxytetrahydropyran in 95% yield, m.p. 103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401751 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-2dfff9b12a674db8b0358460a6ef888f |
| Source note | uspto-grants-1995_03 |