Methanol → HCID 20081868, compound

HRID 1609569Notes

Reaction equation

HRID 1609569 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:13]([CH:14]=[O:15])=[C:12]([CH:16]([CH3:18])[CH3:17])[C:11]([CH2:19][OH:20])=[C:10]([CH:21]([CH3:23])[CH3:22])[N:9]=2)=[CH:4][CH:3]=1.[CH3:24]O>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:13]([CH:14]=[O:15])=[C:12]([CH:16]([CH3:18])[CH3:17])[C:11]([CH2:19][O:20][CH3:24])=[C:10]([CH:21]([CH3:23])[CH3:22])[N:9]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 887MethanolHCID 20081803HCID 20081803, compound

Product 1

HCID 20081868HCID 20081868, compound

Procedure

3.15 g (96% of theory) of colorless crystals of m.p. 77° C. (from MeOH) are obtained from 3.15 g (10 mmol) of the compound from Example 122 in analogy to the instructions from Example 59

Sources & evidence

ORD record
ord-ef72ae071cf84a53be4969bc4aae0417
Source dataset
uspto-grants-1995_03
Patent number
US05401746

Reaction notes

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