Acetic Acid → HCID 15230472, compound

Participants

Reaction Steps

To a mixture of 870 mg of 4-(4-chlorobenzoyl)phthalic acid anhydride, 10 ml of acetic acid and 10 ml of toluene was added 394 mg of 3-aminomethylpyridine, and the resultant mixture was refluxed under heating for 2 hours. The reaction mixture was concentrated in vacuo, and the resultant residue was chromatographed on a column of silica gel, eluting with ethyl acetate to give 1.11 g of the titled compound.

Provenance & Evidence