HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9817693, compound → HCID 19046557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9817693 | HCID 9817693 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19046557 | HCID 19046557 | — |
Reaction Steps
To a solution of 220 mg of 1-(2-dimethylaminoethyl)-1-(3,4,5-trimethoxyphenyl)urea in a mixture of ethanol (3 ml) and diethyl ether (15 ml) was added 4N-HCl-dioxane dropwise with stirring. The resulting crystals were collected by filtration and dried under reduced pressure to provide 230 mg of 1-(2-dimethylaminoethyl)-1-(3,4,5-trimethoxyphenyl)urea hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401775 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-8f11386c2e784df595d1489656cf7ed2 |
| Source note | uspto-grants-1995_03 |