HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[6-Fluoro-2-methyl-3-[(4-methylsulfonylphenyl)methylidene]inden-1-yl]acetic acid → Sodium 5-fluoro-2-methyl-1-(rho-methylsulfonylbenzylidene)-3-indenylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[6-Fluoro-2-methyl-3-[(4-methylsulfonylphenyl)methylidene]inden-1-yl]acetic acid | HCID 114866 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sodium 5-fluoro-2-methyl-1-(rho-methylsulfonylbenzylidene)-3-indenylacetate | HCID 70149782 | — |
Reaction Steps
5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetic acid (1.79 g.) in methanol (10 ml.) is added to a solution of sodium methoxide (0.27 g.) in methanol (5 ml.). The reaction mixture is stirred for 20 minutes and evaporated to dryness to yield sodium 5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401774 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-0a41e06d20794d9db99ccf3ec368d4b8 |
| Source note | uspto-grants-1995_03 |