HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → 2-Tertbutoxycarbonylamino-7-vinyl-tetraline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | (2R)2-tertbutoxycarbonylamino-7-trifluoromethanesulfonyloxy-tetraline | HCID 18651770 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Tertbutoxycarbonylamino-7-vinyl-tetraline | HCID 19386051 | — |
Reaction Steps
The compound is obtained by following the procedure described in Preparation I step b) but starting from the product obtained in step b) above. Yield: 7 g. M.p. 89°-91° C. (isopropyl ether). [α]D20 =+40° (c=0.3%, CH2Cl2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401879 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-4da80e8ae7464a53948a87cc851ddcda |
| Source note | uspto-grants-1995_03 |