Formaldehyde → HCID 22262370, compound

Participants

Reaction Steps

In a similar manner to Example 1, 202.1 g (0.75 mol) of diisononylamine and 170.3 g (1.65 mol) of formaldehyde (29.1%) are reacted in a 1 l autoclave; a maximum pressure of 1.9 MPa is established at a temperature of 160° C. After the end of the reaction, the organic phase is removed from the aqueous phase; the remaining organic phase is subsequently distilled. 208.0 g of N-methyldiisononylamine having a purity of 85.0% are isolated, corresponding to a yield of 83.2% of theory.

Provenance & Evidence