Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(1-Naphthalenyl)-2-propenoic acid → 1-Naphthalenepropionic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(1-Naphthalenyl)-2-propenoic acid | HCID 98307 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-Naphthalenepropionic acid | HCID 95254 | 99% |
반응 단계
10% Palladium on carbon (1.00 g) was added to a suspension of 3-(1-naphthyl)acrylic acid (50.0 g) in tetrahydrofuran (500 ml). The mixture was hydrogenated at 6 atmospheres for 18 hours then filtered through a kieselguhr pad washing with ethyl acetate (3×10 ml). The filtrate was evaporated under reduced pressure to give the subtitle compound (50.0 g) as a solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06984644B2 |
| 출처 데이터셋 | uspto-grants-2006_01 |
| ORD ID | ord-5673ec474f694bc49623cf8b3c0713f0 |
| 출처 메모 | uspto-grants-2006_01 |