5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione → HCID 15957705, compound

HRID 1611268Notes

Reaction equation

HRID 1611268 reaction equation
[CH:1]([C:4]1[C:5](=[O:20])[NH:6][C:7](=[O:19])[NH:8][C:9]=1[S:10][C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[CH:12]=1)([CH3:3])[CH3:2].[C:21]1([CH3:38])[CH:26]=[CH:25][C:24](S(OCC2CCCCC2)(=O)=O)=[CH:23][CH:22]=1>>[CH:21]1([CH2:38][N:8]2[C:9]([S:10][C:11]3[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=3)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:20])[NH:6][C:7]2=[O:19])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1

Participants

3

Reactant 2

HCID 104937275-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedioneHCID 11807699Cyclohexylmethyl 4-methylbenzenesulfonate

Product 1

HCID 15957705HCID 15957705, compoundYield 54.3%

Procedure

5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione and (cyclohexyl)methyl para-toluenesulfonate were reacted by the same way with the example 1 to obtain the titled compound (210 mg, yield: 54.3%).

Sources & evidence

ORD record
ord-b380a81ee1aa404c874479fc7ad8974a
Source dataset
uspto-grants-2006_01
Patent number
US06987114B1

Reaction notes

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