5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione → HCID 9906712, compound

HRID 1611269Notes

Reaction equation

HRID 1611269 reaction equation
[CH2:1]([C:3]1[C:4](=[O:19])[NH:5][C:6](=[O:18])[NH:7][C:8]=1[O:9][C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[C:12]([CH3:17])[CH:11]=1)[CH3:2].[C:20]1([CH3:37])[CH:25]=[CH:24][C:23](S(OCC2CCCCC2)(=O)=O)=[CH:22][CH:21]=1>>[CH:20]1([CH2:37][N:7]2[C:8]([O:9][C:10]3[CH:11]=[C:12]([CH3:17])[CH:13]=[C:14]([CH3:16])[CH:15]=3)=[C:3]([CH2:1][CH3:2])[C:4](=[O:19])[NH:5][C:6]2=[O:18])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1

Participants

3

Reactant 2

HCID 109232665-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedioneHCID 11807699Cyclohexylmethyl 4-methylbenzenesulfonate

Product 1

HCID 9906712HCID 9906712, compoundYield 51.9%

Procedure

5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione and (cyclohexyl)methyl para-toluenesulfonate were reacted by the same way with the example 1 to obtain the titled compound (185 mg, yield: 51.9%).

Sources & evidence

ORD record
ord-54ce1d77827644658cea6abbd02b45d7
Source dataset
uspto-grants-2006_01
Patent number
US06987114B1

Reaction notes

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