3,5-Dimethoxybenzyl Bromide → HCID 15957741, compound

HRID 1611311Notes

Reaction equation

HRID 1611311 reaction equation
[CH:1]([C:4]1[C:5](=[O:21])[NH:6][C:7](=[O:20])[NH:8][C:9]=1[C:10](=[O:19])[C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[CH:12]=1)([CH3:3])[CH3:2].[CH3:22][O:23][C:24]1[CH:25]=[C:26]([CH:29]=[C:30]([O:32][CH3:33])[CH:31]=1)[CH2:27]Br>>[CH3:33][O:32][C:30]1[CH:29]=[C:26]([CH:25]=[C:24]([O:23][CH3:22])[CH:31]=1)[CH2:27][N:8]1[C:9]([C:10](=[O:19])[C:11]2[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=2)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:21])[NH:6][C:7]1=[O:20]

Participants

3

Reactant 2

HCID 12744903,5-Dimethoxybenzyl BromideHCID 222565826-(3,5-Dimethyl-benzoyl)-5-isopropyl-1H-pyrimidine-2,4-dione

Product 1

HCID 15957741HCID 15957741, compoundYield 67.8%

Procedure

5-Isopropyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and 3,5-dimethoxybenzyl bromide were reacted by the same way with the example 1 to obtain the titled compound (296 mg, yield: 67.8%).

Sources & evidence

ORD record
ord-73b1ba994f5e4ece87f47fe3fc1ee0b1
Source dataset
uspto-grants-2006_01
Patent number
US06987114B1

Reaction notes

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