HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dibromobenzyl bromide → 1-(3,5-Dibromobenzyl)-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dibromobenzyl bromide | HCID 143427 | — |
| Reactant | 6-(3,5-dimethylbenzoyl)-5-ethylpyrimidine-2,4(1H,3H)-dione | HCID 22256579 | — |
| Product | 1-(3,5-Dibromobenzyl)-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione | HCID 15957765 | 74.4% |
Reaction Steps
5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and 3,5-dibromobenzyl bromide were reacted by the same way with the example 1 to obtain the titled compound (387 mg, yield: 74.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06987114B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-b8dc34000903409c9806cd72eadd5579 |
| Source note | uspto-grants-2006_01 |