Allyl bromide → HCID 22256584, compound

HRID 1611372Notes

Reaction equation

HRID 1611372 reaction equation
[CH2:1]([C:3]1[C:4](=[O:20])[NH:5][C:6](=[O:19])[NH:7][C:8]=1[C:9](=[O:18])[C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[C:12]([CH3:17])[CH:11]=1)[CH3:2].[CH2:21](Br)[CH:22]=[CH2:23]>>[CH2:23]([N:7]1[C:8]([C:9](=[O:18])[C:10]2[CH:11]=[C:12]([CH3:17])[CH:13]=[C:14]([CH3:16])[CH:15]=2)=[C:3]([CH2:1][CH3:2])[C:4](=[O:20])[NH:5][C:6]1=[O:19])[CH:22]=[CH2:21]

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 222565796-(3,5-dimethylbenzoyl)-5-ethylpyrimidine-2,4(1H,3H)-dione

Product 1

HCID 22256584HCID 22256584, compoundYield 60.8%

Procedure

5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and allyl bromide were reacted by the same way with the example 45-1 to obtain the titled compound (190 mg, yield: 60.8%).

Sources & evidence

ORD record
ord-51cb55870cf44341a88e56c0a5643bb5
Source dataset
uspto-grants-2006_01
Patent number
US06987114B1

Reaction notes

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