HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22254626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-Methyl-8-hydroxyquinoline | HCID 13224 | — |
| Reactant | 2-Amino-8-quinolinol | HCID 4653788 | — |
| Product | HCID 22254626 | HCID 22254626 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 86 substituting 2-aminoquinolin-8-ol for 8-hydroxyquinaldine. 1H NMR (500 MHz, CDCl3) δ ppm 7.99 (m, 2H), 7.33 (m, 3H), 7.22 (m, 2H), 7.14 (m, 2H), 7.08 (m, 1H), 4.69 (m, 1H), 4.23 (m, 2H), 1.88 (m, 4H), 1.46 (d, 3H); MS (DCI/NH3) m/z 389 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-45505bd204ea4892b50d58ce7f72bf3a |
| Source note | uspto-grants-2006_01 |