HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 9998139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Guaiacol | HCID 460 | — |
| Reactant | 2-Methyl-8-hydroxyquinoline | HCID 13224 | — |
| Product | HCID 9998139 | HCID 9998139 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 86 substituting 2-methoxyphenol for 8-hydroxyquinaldine. 1H NMR (500 MHz, CDCl3) δ ppm 7.94 (d, 1H), 7.28 (t, 1H), 7.15 (m, 1H), 7.14 (d, 1H), 7.02 (d, 1H), 6.86 (m, 4H), 4.74 (m, 1H), 4.06 (m, 2H), 3.80 (m, 3H), 2.21 (m, 1H), 2.02 (m, 3H), 1.45 (d, 3H); MS (DCI/NH3) m/z 353 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-76cc254574754f69ba98d9770ca79989 |
| Source note | uspto-grants-2006_01 |