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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1611683Generated: November 1, 2026

Ammonia → HCID 9998139, compound

https://huagongshe.com/reaction/1611683

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantGuaiacolHCID 460—
Reactant2-Methyl-8-hydroxyquinolineHCID 13224—
ProductHCID 9998139HCID 9998139—

Reaction Steps

The title compound was prepared according to the procedure described in Example 86 substituting 2-methoxyphenol for 8-hydroxyquinaldine. 1H NMR (500 MHz, CDCl3) δ ppm 7.94 (d, 1H), 7.28 (t, 1H), 7.15 (m, 1H), 7.14 (d, 1H), 7.02 (d, 1H), 6.86 (m, 4H), 4.74 (m, 1H), 4.06 (m, 2H), 3.80 (m, 3H), 2.21 (m, 1H), 2.02 (m, 3H), 1.45 (d, 3H); MS (DCI/NH3) m/z 353 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06989392B2
Source datasetuspto-grants-2006_01
ORD IDord-76cc254574754f69ba98d9770ca79989
Source noteuspto-grants-2006_01