Ammonia → HCID 22254564, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Example 86 substituting 7-hydroxyquinoline for 8-hydroxyquinaldine. 1H NMR (500 MHz, CDCl3) δ ppm 8.99 (br d, 1H), 8.61 (d, 1H), 7.88 (d, 1H), 7.83 (d, 1H), 7.77 (d, 1H), 7.65 (dd, 1H), 7.30 (m, 2H), 7.19 (m, 1H), 7.14 (d, 1H), 7.01 (d, 1H), 4.73 (m, 1H), 4.22–4.42 (m, 2H), 2.19 (m, 2H), 2.00 (m, 2H), 1.48 (d, 3H); MS (DCI/NH3) m/z 373 [M+H]+.

Provenance & Evidence