HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22252724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 22252742 | HCID 22252742 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | HCID 22252724 | HCID 22252724 | — |
Reaction Steps
In a manner similar to that of Example 2, by reaction of 312 mg (0.49 mmol) of ethyl 6-[3-[5-(tert-butyldimethylsilanyloxy)pentyloxy]-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylselanyl]nicotinate with 213 mg (5.3 mmol) of sodium hydroxide in a THF/ethanol mixture (5 ml/5 ml), 210 mg (71%) of a yellow powder are obtained. m.p.: 161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992094B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-c685b36770d1490b9773642b1c31cbc8 |
| Source note | uspto-grants-2006_01 |