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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1612022Generated: November 4, 2026

Potassium Carbonate → HCID 22252712, compound

https://huagongshe.com/reaction/1612022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantEthyl 4-bromobutyrateHCID 76300—
ReactantHCID 22252718HCID 22252718—
SolventMethyl Ethyl KetoneHCID 6569—
ProductHCID 22252712HCID 22252712—

Reaction Steps

In a manner similar to that of Example 51, by reaction of 300 mg (0.86 mmol) of ethyl 4-(3-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl selanyl)benzoate with 336 mg (1.72 mmol) of ethyl 4-bromobutanoate and 238 mg of potassium carbonate in MEK (10 ml), 364 mg (78%) of a yellow oil are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06992094B1
Source datasetuspto-grants-2006_01
ORD IDord-74322265f2d04b2292604db10e8807da
Source noteuspto-grants-2006_01