HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Benzyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | Benzyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1) | HCID 22253144 | — |
Reaction Steps
From benzyl alcohol (50 ml) and 5-amino-4-oxopentanoic acid hydrochloride (10.0 g; 60 mmol). After 23 h at 90°, excess benzyl alcohol was distilled off at 90° (bath temperature) and 0.33 mm Hg. The yield was 8.1 g (53%) of tan powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992107B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-21ec068a2301477da971fe7d91c3518c |
| Source note | uspto-grants-2006_01 |