Chroman-4-one oxime → (NZ)-N-(5-ethyl-6,7-dihydro-5H-1-benzofuran-4-ylidene)hydroxylamine

Participants

Reaction Steps

Following the procedure for the preparation of (4E)-2,3-dihydro-4H-chromen-4-one oxime but substituting 5-ethyl-6,7-dihydro-1-benzofuran-4(5H)-one and making non-critical variations provided the title compound as a oil: MS (EI) m/z (rel. intensity) 179 (M+, 21), 162 (50), 151 (43), 135 (99), 134 (99), 107 (86), 106 (83), 84 (34), 79 (35), 52 (47), 51(48). HRMS (FAB) calcd for C10H13NO2+H 180.1024, found 180.1015.

Provenance & Evidence