HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiochroman-4-one → 3,4-dihydro-2H-thiochromen-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiochroman-4-one | HCID 19048 | — |
| Reactant | 4,5,6,7-Tetrahydro-1-benzofuran-4-amine | HCID 18525171 | — |
| Product | 3,4-dihydro-2H-thiochromen-4-amine | HCID 85921 | — |
Reaction Steps
Following the procedure for the preparation of 4,5,6,7-tetrahydro-1-benzofuran-4-amine but substituting 2,3-dihydro-4H-thiochromen-4-one and making non-critical variations provided the title compound as a oil: 1H NMR (300 MHz, CDCl3) δ 7.30, 7.07, 4.07, 3.28, 2.96, 2.16, 1.61; (MS/CI) calcd for C9H11NS+H 166.3, found 166.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992087B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-60d73d4c3400429db0dab59504d83f1e |
| Source note | uspto-grants-2006_01 |