Iodoethane → 2-Ethyl-6-methoxyindan-1-one

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Iodoethane	HCID 6340	—
Edukt	6-Methoxy-alpha-tetralone	HCID 14112	—
Edukt	5-propyl-6,7-dihydro-1-benzothiophen-4(5H)-one	HCID 22147491	—
Produkt	2-Ethyl-6-methoxyindan-1-one	HCID 21840579	—

Reaktionsschritte

Following the procedure for the preparation of 5-propyl-6,7-dihydro-1-benzothiophen-4(5H)-one but substituting 6-methoxy 1-tetralone and ethyl iodide, and making non-critical variations provided the title compound as a oil: 1H NMR (CDCl3) δ 1.02, 1.55, 1.99, 2.68, 2.77, 3.27, 3.86, 7.21, 7.37; HRMS (FAB) calcd for C12H14O2+H 191.1072, found 191.1075.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06992087B2
Quelldatensatz	uspto-grants-2006_01
ORD ID	ord-f1de98454b9b4a22b85de92a13af9590
Quellennotiz	uspto-grants-2006_01