HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chroman-4-one oxime → 2-ethyl-6-methoxy-2,3-dihydro-1H-inden-1-one oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chroman-4-one oxime | HCID 9673039 | — |
| Reactant | 2-Ethyl-6-methoxyindan-1-one | HCID 21840579 | — |
| Product | 2-ethyl-6-methoxy-2,3-dihydro-1H-inden-1-one oxime | HCID 73867080 | — |
Reaction Steps
Following the procedure for the preparation of (4E)-2,3-dihydro-4H-chromen-4-one oxime but substituting 2-ethyl-6-methoxyindan-1-one and making non-critical variations provided the title compound as a oil: HRMS (FAB) calcd for C12H15NO2+H 206.1181, found 206.1175. Anal. Calcd for C12H15NO2: C, 70.22; H, 7.37; N, 6.82. Found: C, 69.90; H, 7.48; N, 6.64.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992087B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-dfaf4f80f2ed45c7b020fe86e523e338 |
| Source note | uspto-grants-2006_01 |