HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,7-Dihydro-5H-1-pyridin-5-one → (5Z)-N-Hydroxy-6,7-dihydro-5H-cyclopenta[b]pyridin-5-imine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,7-Dihydro-5H-1-pyridin-5-one | HCID 1512521 | — |
| Reactant | Chroman-4-one oxime | HCID 9673039 | — |
| Product | (5Z)-N-Hydroxy-6,7-dihydro-5H-cyclopenta[b]pyridin-5-imine | HCID 45079548 | — |
Reaction Steps
Following the procedure for the preparation of (4E)-2,3-dihydro-4H-chromen-4-one oxime but substituting 6,7-dihydro-5H-cyclopenta[b]pyridin-5-one and making non-critical variations provided the title compound as a oil: 1H NMR (400 MHz, DMSO-d6) δ) 11.11, 8.50, 7.89, 7.27, 3.04, 2.81; HRMS (EI) calcd for C8H8N2O 148.0637, found 148.0628.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992087B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-5a92c95669d54213ae0ea79459ab03aa |
| Source note | uspto-grants-2006_01 |