Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodoethane → Ethyl-1-indanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | 1-Tetralone | HCID 10724 | — |
| 반응물 | 5-propyl-6,7-dihydro-1-benzothiophen-4(5H)-one | HCID 22147491 | — |
| 생성물 | Ethyl-1-indanone | HCID 5070076 | — |
반응 단계
Following the procedure for the preparation of 5-propyl-6,7-dihydro-1-benzothiophen-4(5H)-one but substituting 1-tetralone and ethyl iodide, and making non-critical variations provided the title compound as a colorless mobile oil. IR (liq.) 2963, 2933, 2875, 2860, 1712, 1610, 1588, 1475, 1464, 1327, 1296, 1278, 1205, 749, 718 cm−1; MS (EI) m/z 160 (M+); Anal. Calcd for C11H12O: C, 82.46; H, 7.55. Found: C, 82.16; H, 7.57.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06992087B2 |
| 출처 데이터셋 | uspto-grants-2006_01 |
| ORD ID | ord-0a35126abc6546bca3c3fcdcfe51028c |
| 출처 메모 | uspto-grants-2006_01 |